Comparison of Ductile-Brittle Transition Temperature Testing of 3Cr1MoV Steel with Small Punch Specimens of Different Notch Forms
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摘要: 将加氢反应器中的3Cr1MoV钢试块加工成直线型U型和V型缺口试样,并在-196~25℃进行小冲杆试验,对比研究了2种缺口形式试样的载荷-位移曲线、断口形貌以及Esp/Fm(Esp为断裂能,Fm为最大载荷)-温度曲线。结果表明:V型缺口试样的载荷-位移曲线在温度低于-140℃下存在pop-in现象;U型缺口试样的载荷-位移曲线光滑,随着温度的降低,其最大载荷先增后降,最大位移减小;在相同试验温度下,2种缺口形式试样的断口形貌差异不大;U型缺口试样的Esp/Fm-温度曲线具有明显的上下平台,其拟合相关系数高于V型缺口试样的,因此U型缺口试样比V型缺口试样更适用于小冲杆试验评估韧脆转变温度。Abstract: Small punch tests at -196-25℃ were carried out on linear-type U-notched and V-notched specimens, which were machined from 3Cr1MoV steel test blocks in a hydrogenation reactor. The load-displacement curves, fracture morphology and Esp/Fm (Esp is fracture energy, Fm is maximum load) vs temperature curves of two notched specimens were compared. The results show that the load-displacement curves of V-notched specimens indicated a pop-in phenomenon below -140℃ while those of U-notched specimens were smooth. With the decrease of temperature, the maximum load of U-notched specimen increased and then decreased, and the maximum displacement decreased. The fracture morphology of two notched specimens had small difference at the same test temperatures. The Esp/Fm vs temperature curve of U-notched specimen had obvious up and down platforms, and the correlation coefficient was higher than that of V-notched specimen, therefore the U-notched specimen is more suitable to evaluate the ductile-brittle transition temperature by small punch test than the V-notched specimen.
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[1] 汪逸安, 谢国山, 钱晓龙. 步冷及充氢对2.25CrlMo钢韧脆转温度的影响[J]. 中国特种设备安全, 2014(1):29-30. [2] 林建鸿, 柳曾典, 吴东棣. 热壁加氢反应器运行过程中的材质劣化问题[J]. 石油化工设备技术, 1997(5):4-9. [3] 杨光起. 加氢反应器用铬钼钢回火脆性[J]. 石油化工设备, 2001, 30(5):53-57. [4] 许立萌, 关凯书. 小冲杆试验测试3Cr1Mo1/4V钢制加氢反应器内试块的回火脆性[J]. 机械工程材料, 2017, 41(5):84-88. [5] TURBA K, HURST R, HÄHNER P. Evaluation of the ductile-brittle transition temperature in the NESC-I material using small punch testing[J]. International Journal of Pressure Vessels and Piping, 2013, 111/112:155-161.
[6] JIA X, DAI Y. Small punch tests on martensitic/ferritic steels F82H, T91 and Optimax-A irradiated in SINQ Target-3[J]. Journal of Nuclear Materials, 2003, 323(2/3):360-367.
[7] 朱锦斌. 环形裂纹小冲杆试样精度确定和试验研究[D]. 上海:华东理工大学, 2016. [8] GVLÇIMEN B, DURMUŞ A, VLKV S, et al. Mechanical characterisation of a P91 weldment by means of small punch fracture testing[J]. International Journal of Pressure Vessels and Piping, 2013, 105/106:28-35.
[9] CUESTA I I, ALEGRE J M. Determination of the fracture toughness by applying a structural integrity approach to pre-cracked small punch test specimens[J]. Engineering Fracture Mechanics, 2011, 78(2):289-300.
[10] CONTRERAS M A, RODRIGUEZ C, BELZUNCE F J, et al. Use of the small punch test to determine the ductile-to-brittle transition temperature of structural steels[J]. Fatigue & Fracture of Engineering Materials & Structures, 2008, 31(9):727-737.
[11] BRUCHHAUSEN M, HOLMSTRÖM S, LAPETITE J M, et al. On the determination of the ductile to brittle transition temperature from small punch tests on Grade 91 ferritic-martensitic steel[J]. International Journal of Pressure Vessels and Piping, 2017, 155:27-34.
[12] MATOCHA K. The use of small punch tests for determination of fracture behaviour of ferritic steels[J]. Procedia Engineering, 2014, 86(4):885-891.
[13] 陈建涛. 小冲杆试验方法评价材料低温力学性能的研究[D]. 上海:华东理工大学, 2012. [14] 付丽秦, 王进, 刘文松, 等. 42CrMo低温冲击韧性研究[J]. 机车车辆工艺, 2017(4):31-33. [15] 梁波, 李杰, 乔志华,等. 35CrNi3MoV钢韧脆转变温度测定[J]. 理化检验-物理分册, 1997,33(2):26-26.
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