• CSCD中国科学引文数据库来源期刊
  • 中文核心期刊
  • 中国机械工程学会材料分会会刊
  • 中国科技核心期刊
高级检索

微米尺度压痕测试设备的研发及其可靠性

伍杰, 孙坤, 马增胜

伍杰, 孙坤, 马增胜. 微米尺度压痕测试设备的研发及其可靠性[J]. 机械工程材料, 2022, 46(2): 88-94. DOI: 10.11973/jxgccl202202014
引用本文: 伍杰, 孙坤, 马增胜. 微米尺度压痕测试设备的研发及其可靠性[J]. 机械工程材料, 2022, 46(2): 88-94. DOI: 10.11973/jxgccl202202014
WU Jie, SUN Kun, MA Zengsheng. Development and Reliability of Micro-Scale Indentation Testing Equipment[J]. Materials and Mechanical Engineering, 2022, 46(2): 88-94. DOI: 10.11973/jxgccl202202014
Citation: WU Jie, SUN Kun, MA Zengsheng. Development and Reliability of Micro-Scale Indentation Testing Equipment[J]. Materials and Mechanical Engineering, 2022, 46(2): 88-94. DOI: 10.11973/jxgccl202202014

微米尺度压痕测试设备的研发及其可靠性

基金项目: 

国家自然科学基金面上资助项目(11872054)

湖南省自然科学基金杰出青年基金资助项目(2020JJ2026)

湖南省教育厅重点项目(19A122)

详细信息
    作者简介:

    伍杰(1982-),男,湖南澧县人,副教授,博士

  • 中图分类号: TH122

Development and Reliability of Micro-Scale Indentation Testing Equipment

  • 摘要: 基于Oliver-Pharr方法和断裂韧度测试方法成功研制了一台微米尺度压痕测试设备,使用有限元方法对其机械可靠性进行验证,并利用该设备测试了高纯铝和氧化锆陶瓷的力学性能参数,验证设备的测试性能。结果表明:所研制的微米尺度压痕测试设备结构稳定,设计合理,闭环控制稳定性好,噪声水平较低,满足测试要求。采用该设备在不同压入载荷下测得高纯铝及氧化锆陶瓷的硬度、弹性模量以及断裂韧度与使用标准压痕设备测试得到的结果一致,相对误差小于7%,证明了该设备测试结果的准确性。
    Abstract: Based on the Oliver-Pharr method and the fracture toughness test method, a micro-scale indentation testing equipment was successfully developed. Its mechanical reliability was verified by the finite element method, and the mechanical property parameters of the high-purity aluminum and zirconia ceramics were tested by the equipment to verify the test performance of the equipment. The results show that the developed micro-scale indentation testing equipment had stable structure, reasonable design, good closed-loop control stability and low noise level, and met the test requirements. The hardness, elastic modulus and fracture toughness of high-purity aluminum and zirconia ceramics measured by this equipment under different indentation loads were consistent with the results obtained by standard indentation equipment, and the relative error was smaller than 7%, which proved the accuracy of the test results of the equipment.
  • [1]

    EVANS A G,CHARLES E A.Fracture toughness determinations by indentation[J].Journal of the American Ceramic Society,1976,59(7/8):371-372.

    [2]

    BELOSLUDTSEV A,YAKIMOV Y,MROCZYŃSKI R,et al.Effect of annealing on optical,mechanical,electrical properties and structure of scandium oxide films[J].Physica Status Solidi (a),2019,216(18):1900122.

    [3] 郑凯.纳米尺度材料在新型太阳能电池中的应用[J].科技创新与应用,2018(22):10-12.

    ZHENG K.Application of nanoscale materials in new solar cells[J].Technology Innovation and Application,2018(22):10-12.

    [4]

    BAE W C,TEMPLE M M,AMIEL D,et al.Indentation testing of human cartilage:Sensitivity to articular surface degeneration[J].Arthritis & Rheumatism,2003,48(12):3382-3394.

    [5]

    WADULLAH H M,AJEEL S, ABBASS M,et al.Corrosion of platinum nanocoatings thin films deposited by sputtering deposition method for medical applications[J].International Journal of Engineering & Technology,2018,7(4.37):63-66.

    [6]

    JIN T,NIU X Y,XIAO G S,et al.Effects of experimental variables on PMMA nano-indentation measurements[J].Polymer Testing,2015,41:1-6.

    [7] 赵宏伟,时月,刘彦超,等.原位微纳米压痕/划痕测试平台:204536102U[P].2015-08-05.

    ZHAO H W,SHI Y,LIU Y C,et al.In situ micro-nano indentation/scratch test platform:204536102U[P].2015-08-05.

    [8] 刘晓坤,蔡力勋,陈辉.获取材料应力应变关系的锥形压入新方法[J].中国测试,2016,42(4):5-8.

    LIU X K,CAI L X,CHEN H.A new conical indentation method for obtaining stress-strain relation of materials[J].China Measurement & Test,2016,42(4):5-8.

    [9] 刘东旭,张泰华,郇勇.宏观深度测量压入仪器的研制[J].力学学报,2007,39(3):350-355.

    LIU D X,ZHANG T H,HUAN Y.Development of macro-depth-sensing-indentation instrumentation[J].Chinese Journal of Theoretical and Applied Mechanics,2007,39(3):350-355.

    [10] 马德军,陈伟.基于单一Vickers压头的材料弹塑性参数仪器化压入测试方法:103411833A[P].2013-11-27.

    MA D J,CHEN W.Instrumentation indentation test method for elastic-plastic parameters of material based on single Vickers pressure head:103411833A[P].2013-11-27.

    [11] 蒋庄德,王海容,赵则祥,等.微机械力学性能测试仪:2412212Y[P].2000-12-27.

    JIANG Z D,ZHAO W H. Micro-mechanical mechanics performance tester:2412212Y[P].2000-12-27.

    [12]

    OLIVER W C,PHARR G M.An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments[J].Journal of Materials Research,1992,7(6):1564-1583.

    [13]

    SNEDDON I N.The relation between load and penetration in the axisymmetric boussinesq problem for a punch of arbitrary profile[J].International Journal of Engineering Science,1965,3(1):47-57.

    [14]

    ZHANG Y,GUO S,GAO W,et al.Mechanical behavior and simulation analysis of micro/nano indentation of single crystal silicon carbide[J].Yadian Yu Shengguang/Piezoelectrics and Acoustooptics,2018,40(5):742-745.

    [15]

    LAWN B R,FULLER E R.Equilibrium penny-like cracks in indentation fracture[J].Journal of Materials Science,1975,10(12):2016-2024.

    [16] 宋仲康,马德军,陈伟,等.基于仪器化压入技术的结构陶瓷材料断裂韧性测试[J].装甲兵工程学院学报,2012,26(2):85-88.

    SONG Z K,MA D J,CHEN W,et al.Test of fracture toughness of structural ceramics based on instrumental indentation technology[J].Journal of Academy of Armored Force Engineering,2012,26(2):85-88.

    [17] 杨伟华,王全胜.等离子喷涂纳米氧化锆涂层性能的试验研究[J].航空制造技术,2004(增刊1):241-243.

    YANG W H,WANG Q S.Experimental study on performance of nanostructured zirconia coatings by plasma spraying[J].Aeronautical Manufacturing Technology,2004(s1):241-243.

计量
  • 文章访问数:  4
  • HTML全文浏览量:  0
  • PDF下载量:  2
  • 被引次数: 0
出版历程
  • 收稿日期:  2021-01-04
  • 修回日期:  2021-12-22
  • 刊出日期:  2022-02-19

目录

    /

    返回文章
    返回