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    王磊, 刘杨, 宋秀, 孙世鑫, 刘世忠, 李嘉荣. 铼含量对第四代镍基单晶高温合金凝固组织的影响[J]. 机械工程材料, 2022, 46(8): 15-21,27. DOI: 10.11973/jxgccl202208003
    引用本文: 王磊, 刘杨, 宋秀, 孙世鑫, 刘世忠, 李嘉荣. 铼含量对第四代镍基单晶高温合金凝固组织的影响[J]. 机械工程材料, 2022, 46(8): 15-21,27. DOI: 10.11973/jxgccl202208003
    WANG Lei, LIU Yang, SONG Xiu, SUN Shixin, LIU Shizhong, LI Jiarong. Effect of Re Content on Solidification Structure of Fourth Generation Nickel-Based Single Crystal Superalloy[J]. Materials and Mechanical Engineering, 2022, 46(8): 15-21,27. DOI: 10.11973/jxgccl202208003
    Citation: WANG Lei, LIU Yang, SONG Xiu, SUN Shixin, LIU Shizhong, LI Jiarong. Effect of Re Content on Solidification Structure of Fourth Generation Nickel-Based Single Crystal Superalloy[J]. Materials and Mechanical Engineering, 2022, 46(8): 15-21,27. DOI: 10.11973/jxgccl202208003

    铼含量对第四代镍基单晶高温合金凝固组织的影响

    Effect of Re Content on Solidification Structure of Fourth Generation Nickel-Based Single Crystal Superalloy

    • 摘要: 以第四代镍基单晶高温合金DD15为基础,将其铼含量(质量分数)分别调整为5%,6%,7%制备单晶高温合金,研究了铼含量对合金凝固组织特征与元素分布的影响。结果表明:随铼含量的增加,试验合金的γ'相析出温度、溶解温度升高,固相线温度略微下降,液相线温度无明显变化;增加铼含量,合金一次枝晶间距与二次枝晶间距均增大,(γ+γ')共晶组织含量增多,γ'相尺寸减小,体积分数降低;铼含量的增加使得合金组织中负偏析元素铼、钨、钼、铬、钴的偏析程度降低,但正偏析元素钽的偏析程度增大。

       

      Abstract: Based on the fourth generation nickel-based single crystal superalloy DD15, single crystal superalloys were prepared by adjusting its Re content (mass fraction) to 5%, 6% and 7%, respectively. The effects of Re content on the solidification microstructure characteristic and element distribution of the alloy were studied. The results show that with increasing Re content, the precipitation temperature and dissolution temperature of γ' phase of the alloy increased, while the solidus temperature decreased slightly and the liquidus temperature had no obvious change. With increasing Re content, both the primary and secondary dendrite spacings increased, the content of (γSymbolk@@γ') eutectic microstructure increased, while the size and volume fraction of γ' phase decreased. Increase in Re content could decrease the segregation degree of negative segregation elements such as Re, W, Mo, Cr and Co in the alloy structure, but increase the segregation degree of the positive segregation element Ta.

       

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