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    不同温度下铁镍基高温合金的蠕变性能及组织演变

    Creep Properties and Microstructure Evolution of Fe-Ni Based Superalloy under Different Temperatures

    • 摘要: 在250 MPa恒拉应力下对铁镍基高温合金开展675 ℃和700 ℃高温蠕变试验,研究了不同温度下试验合金的蠕变性能及蠕变断裂后的显微组织。结果表明:不同温度下蠕变后试验合金的蠕变断裂方式均为沿晶断裂,700 ℃下的蠕变寿命比675 ℃下缩短7 891 h,700 ℃下试验合金的过早断裂与其组织中形成较多不均匀分布的位错缠结有关。675 ℃蠕变后试验合金的晶粒尺寸明显大于700 ℃蠕变后,且晶粒尺寸分布更分散。与675 ℃蠕变后相比,700 ℃蠕变后试验合金中TiC尺寸较大,且趋于团聚或呈条带状分布,Cr23C6的平均宽度较小;不同温度蠕变后的Cr23C6碳化物均未形成明显的连续网状结构;不同温度蠕变后晶粒内γ′相呈球形,675 ℃下γ′相平均尺寸更大;不同温度蠕变后试验合金晶界上均存在极少量无析出区和不连续粗化区。

       

      Abstract: High-temperature creep tests at 675 ℃ and 700 ℃ were conducted on Fe-Ni based superalloy under a constant tensile stress of 250 MPa. The creep properties and microstructure after creep fracture of the test alloy at different temperatures were studied. The results show that the creep fracture mode of the test alloy after creep at different temperatures was intergranular fracture. The creep life at 700 ℃ was 7 891 h shorter than that at 675 ℃. The premature fracture at 700 ℃ of the test alloy was related to many unevenly distributed dislocation entanglements formed in the microstructure. The grain size of the test alloy after creep at 675 ℃ was significantly larger than that at 700 ℃, and the grain size distribution was more dispersed. Compared with those after creep at 675 ℃, TiC in the test alloy after creep at 700 ℃ was larger in size and tended to aggregate or be distributed by bands, while the average width of Cr23C6 was smaller. No obvious continuous network structure of Cr23C6 was formed after creep at different temperatures. The γ′ phase within the grains after creep at different temperatures was spherical, and the average size of the γ′ phase after creep at 675 ℃ was relatively large. After creep at different temperatures, there were a very small number of precipitation-free zones and discontinuous coarsening zones on grain boundaries of the test alloy.

       

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