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    TiN对AZ61镁合金显微组织和拉伸性能的影响

    Effect of TiN on Microstructure and Tensile Properties of AZ61 Magnesium Alloy

    • 摘要: 通过在AZ61镁合金中添加质量分数0.5% TiN,研究了TiN对铸态及挤压态AZ61镁合金显微组织和拉伸性能的影响。结果表明:添加TiN后铸态和挤压态AZ61镁合金晶界处出现TiN颗粒,TiN未与其他元素发生化学反应;添加TiN后铸态合金晶粒尺寸由243.2 µm减小到90.2 µm,挤压态合金晶粒尺寸由8.1 µm减小到5.1 μm;添加TiN后,合金中第二相含量明显增多,挤压过程中晶粒的动态再结晶行为受到抑制,组织中出现不完全动态再结晶晶粒;添加TiN后铸态合金的抗拉强度、断后伸长率、屈服强度分别降低了38.3%,31.3%,30.0%,挤压态合金的抗拉强度、断后伸长率、屈服强度分别降低了3.3%,3.7%,28.3%,拉伸性能的降低与硬度较高TiN相在晶界处的偏聚、孪晶的产生、施密特因子的降低和织构的增强有关。

       

      Abstract: The effects of TiN on the microstructure and tensile properties of as-cast and extruded AZ61 magnesium alloy were studied by adding TiN with a mass fraction of 0.5% to the AZ61 magnesium alloy. The results show that after adding TiN, TiN particles appeared at the grain boundaries of the as-cast and extruded AZ61 magnesium alloy, and TiN did not undergo a chemical reaction with other elements. After adding TiN, the grain size of the as-cast alloy decreased from 243.2 µm to 90.2 µm, and that of the extruded alloy decreased from 8.1 µm to 5.1 µm. After adding TiN, the content of the second phase in the alloy increased significantly, the dynamic recrystallization behavior of the grains during the extrusion was inhibited, and incomplete dynamic recrystallization grains appeared in the microstructure. After adding TiN, the tensile strength, percentage elongation after fracture, and yield strength of the as-cast alloy decrease by 38.3%, 31.3%, 30.0%, and those of the extruded alloy decrease by 3.3%, 3.7%, 28.3%, respectively. The decrease in tensile properties was related to the segregation of the hard TiN phase at the grain boundaries, the generation of twins, the decrease in the Schmid factor, and the enhancement of the texture.

       

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