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    扫描速度对选区激光熔化成形GH4169合金微观结构和力学性能的影响

    Effect of Scanning Speed on Microstructure and Mechanical Properties of GH4169 Alloy Formed by Selective Laser Melting

    • 摘要: 采用选区激光熔化(SLM)技术制备GH4169高温合金,研究了扫描速度(600,800,1 000,1 200,1 400 mm·s−1)对SLM成形合金的物相组成、微观结构、显微硬度的影响以及最佳扫描速度下的高温拉伸性能。结果表明:扫描速度对SLM成形合金的物相组成无显著影响;随着扫描速度的增加,合金的孔隙率先降后增,在1 000 mm·s−1扫描速度下达到最小,仅为0.01%,致密性最好。不同扫描速度下合金纵截面熔池交替分布形成鱼鳞形状;600,800 mm·s−1扫描速度下合金纵截面存在不规则熔池及圆形冶金气孔,随着扫描速度增加,熔池边界形貌得到明显改善,1 000 mm·s−1扫描速度下获得具有规则熔池形貌与近全致密组织的合金,1 400 mm·s−1扫描速度下合金中形成大量不规则未熔合孔。不同扫描速度下SLM成形合金的显微硬度在300~360 HV范围,随着扫描速度的增加,合金的硬度基本呈先降后升的趋势,在1 000 mm·s−1扫描速度下硬度最低,约为307 HV。SLM成形GH4169合金的最佳扫描速度为1 000 mm·s−1,随着拉伸试验温度由20 ℃升温至600 ℃,屈服强度和抗拉强度仅降低12%和13%,除500 ℃外断后伸长率均超过10%,拉伸断口均呈韧性断裂形貌。

       

      Abstract: GH4169 superalloy was prepared by selective laser melting (SLM), and the effect of scanning speed (600, 800, 1 000, 1 200, 1 400 mm·s−1) on the phase composition, microstructure and microhardness and the high temperature tensile properties under the optimal scanning speed of the SLM formed alloy were investigated. The results show that the scanning speed had no significant effect on the phase composition of the SLM formed alloy. As the scanning speed increased, the porosity of the alloy first decreased and then increased, and reached the minimum value of only 0.01% under scanning speed of 1 000 mm·s-1, indicating the best densification. The molten pools in the longitudinal section of the alloy were alternately distributed to form a fish-scale shape under different scanning speeds. Under scanning speeds of 600, 800 mm·s−1, there were irregular molten pools and circular metallurgical pores in the longitudinal section of the alloy. With the increase of scanning speed, the morphology of the molten pool boundary was significantly improved. Under scanning speed of 1 000 mm·s−1, the alloy with regular molten pool morphology and nearly fully dense structure was obtained. A large number of irregular unfused pores were formed in the alloy under scanning speed of 1 400 mm·s−1. The microhardness of SLM formed alloy under different scanning speeds ranged from 300 HV to 360 HV. With the increase of scanning speed, the hardness of the alloy basically first decreased and then increased. The hardness was the lowest under scanning speed of 1 000 mm·s−1, approximately 307 HV. The optimal scanning speed for SLM forming of GH4169 alloy was 1 000 mm·s−1; as the tensile test temperature increased from 20 ℃ to 600 ℃, the yield strength and tensile strength only decrease by 12% and 13%, respectively; except for 500 ℃, the percentage elongation after fracture exceeded 10%, and the tensile fracture all showed ductile fracture morphology.

       

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