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    王美娜, 丘泰, 沈春英. 钛酸镁基介电陶瓷的微波烧结[J]. 机械工程材料, 2009, 33(1): 23-25.
    引用本文: 王美娜, 丘泰, 沈春英. 钛酸镁基介电陶瓷的微波烧结[J]. 机械工程材料, 2009, 33(1): 23-25.
    WANG Mei-na, QIU Tai, SHEN Chun-ying. Microwave Sintering of Magnesium Titanate Dielectric Ceramics[J]. Materials and Mechanical Engineering, 2009, 33(1): 23-25.
    Citation: WANG Mei-na, QIU Tai, SHEN Chun-ying. Microwave Sintering of Magnesium Titanate Dielectric Ceramics[J]. Materials and Mechanical Engineering, 2009, 33(1): 23-25.

    钛酸镁基介电陶瓷的微波烧结

    Microwave Sintering of Magnesium Titanate Dielectric Ceramics

    • 摘要: 首先采用固相反应法分别合成了Mg2TiO4和CaTiO3粉体,然后在其混合物(质量比0.95∶0.05)加入质量分数为1.5%的CuO作为烧结助剂进行微波烧结;用排水法、阻抗分析、XRD、SEM等方法对烧结体的密度、电容及介电损耗、晶相组成、微观形貌进行了分析.结果表明:微波烧结明显缩短了烧结周期,并且烧结体的烧结性能和介电性能良好,在1 310 ℃保温45 min获得烧结体的介电性能优异,在10 kHz下介电常数为19.19,介电损耗为0.002 2;烧结体主晶相为Mg2TiO4,次晶相为CaTiO3,同时含有少量的MgTiO3,微波烧结材料中的次晶相发育不完整.

       

      Abstract: First Mg2TiO4 and CaTiO3 powders were prepared by solid state reaction method,and then they were sintered in the microwave stove with 1.5wt% CuO as sintering additives.Density,capacity,dielectric loss,crystal composition and microstructure of the sintering body were ananlyzed by means of Archimedes drainage method,resistance analysis,XRD and SEM.The results showed that microwave sintering technology shortened the sintering period obviously and possessed the sintering body with good sintering and dielectric properties.When sintered at 1 310 ℃ for 45 min,the sintering body had good dielectric properties with dielectric constant of 19.19 and dielectric loss of 0.002 2.The major phase of the sintering body was Mg2TiO4,the second phase was CaTiO3 which growed poorly when sintered by microwave,and a small amount of MgTiO3 had been found at the same time.

       

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