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    吕宝华, 李玉珍, 黄健, 任晓娟. 锡掺杂量对In2O3粉体光学性能和形貌的影响[J]. 机械工程材料, 2015, 39(1): 49-51.
    引用本文: 吕宝华, 李玉珍, 黄健, 任晓娟. 锡掺杂量对In2O3粉体光学性能和形貌的影响[J]. 机械工程材料, 2015, 39(1): 49-51.
    Lv Bao-hua, LI Yu-zhen, HUANG Jian, REN Xiao-juan. Effects of Sn-doping Amounts on Optical Properties and Morphology of In2O3 Powders[J]. Materials and Mechanical Engineering, 2015, 39(1): 49-51.
    Citation: Lv Bao-hua, LI Yu-zhen, HUANG Jian, REN Xiao-juan. Effects of Sn-doping Amounts on Optical Properties and Morphology of In2O3 Powders[J]. Materials and Mechanical Engineering, 2015, 39(1): 49-51.

    锡掺杂量对In2O3粉体光学性能和形貌的影响

    Effects of Sn-doping Amounts on Optical Properties and Morphology of In2O3 Powders

    • 摘要: 采用固相反应法在800℃烧结制备出了不同锡掺杂量的(In1-xSnx)2O3(x=0,0.01,0.02,0.05)粉体,通过X射线衍射仪(XRD)、拉曼光谱仪、傅里叶红外光谱仪(IR)、紫外吸收可见光谱(Uv-vis)分析仪以及扫描电镜(SEM)等对(In1-xSnx)2O3粉体的结构、光学性能和形貌进行了表征。结果表明:不同锡掺杂量的(In1-xSnx)2O3粉体都保持了In2O3的立方相晶胞结构;锡的掺杂改变了In2O3的紫外-可见吸收性能和红外吸收性能,抑制了In2O3粉体颗粒的长大,使其结构变得更加紧密。

       

      Abstract: (In1-xSnx)2O3(x=0,0.01,0.02,0.05)powders with different Sn-doping amounts were prepared by solid state reaction at 800 ℃. The structure,optical properties and morphology of (In1-xSnx)2O3 powders were characterized by X-ray diffraction(XRD),Raman spectroscopy,Fourier transform Tnfrared (IR) spectroscopy,ultraviolet visible (Uv-vis) absorption spectrophotoscopy and scanning electron microscopy(SEM) in detail. The results show that all the (In1-xSnx)2O3 powders with different Sn-doping amounts remained the cubic crystal structure of indium oxide,and its UV-vis and IR absorption properties were changed by the Sn-doping,the growth of In2O3 particles was restrained,and thus their structure became more closely.

       

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