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    王玉雷, 李子全, 刘劲松. 退火温度对NiTi/Si膜结晶特性及力学性能的影响[J]. 机械工程材料, 2010, 34(9): 20-22.
    引用本文: 王玉雷, 李子全, 刘劲松. 退火温度对NiTi/Si膜结晶特性及力学性能的影响[J]. 机械工程材料, 2010, 34(9): 20-22.
    WANG Yu-lei, LI Zi-quan, LIU Jin-song. Effect of Annealing Temperature on Crystallization Characteristics and Mechanical Properties of NiTi/Si Films[J]. Materials and Mechanical Engineering, 2010, 34(9): 20-22.
    Citation: WANG Yu-lei, LI Zi-quan, LIU Jin-song. Effect of Annealing Temperature on Crystallization Characteristics and Mechanical Properties of NiTi/Si Films[J]. Materials and Mechanical Engineering, 2010, 34(9): 20-22.

    退火温度对NiTi/Si膜结晶特性及力学性能的影响

    Effect of Annealing Temperature on Crystallization Characteristics and Mechanical Properties of NiTi/Si Films

    • 摘要: 采用射频磁控溅射法在NiTi膜表面沉积一层非晶硅膜而形成NiTi/Si膜,并对该膜进行了不同温度的退火处理;用XRD、SEM和纳米压痕仪研究了退火温度对NiTi/Si膜的结晶特性和力学性能的影响.结果表明:NiTi/Si膜在600 ℃下退火后其中的硅仍为非晶态;当退火温度在650 ℃后开始出现明显的结晶硅衍射峰,且随着温度升高,硅的结晶度增大,晶粒逐渐长大;而该膜的硬度和抗压痕蠕变能力逐渐降低;该膜弹性模量在650 ℃退火后最大.

       

      Abstract: The amorphous Si films were deposited on NiTi films by radio frequency magnetron sputtering,then annealed at different temperatures.The effect of annealing temperature on the crystallization characteristics and mechanical properties of the NiTi/Si films was studied by XRD,SEM and nano-hardness tester.The results indicate that the Si in the NiTi/Si fims remained amorphous after annealing at 600 ℃,and obvious crystal silicon diffraction peaks ocuured above 650 ℃.The crystallinity and grain size of Si increased,the hardness and indentation creep resistance of the films decreased with increasing annealing temperature.The maximum elastic modulus could be obtained after annealing at 650 ℃.

       

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