Solvothermal Synthesis of Mesoporous Ag<sub>3</sub>VO<sub>4</sub> Powder and Its Photoluminescence Property

LI Yingjie; ZHU Lihua; L&#220; Renjiang; ZHAO Nan; ZHENG Weiwei; WANG Yujia

doi:10.11973/jxgccl201708008

Materials and Mechanical Engineering > 2017 > 41(8): 35-39. > DOI: 10.11973/jxgccl201708008

LI Yingjie, ZHU Lihua, LÜ Renjiang, ZHAO Nan, ZHENG Weiwei, WANG Yujia. Solvothermal Synthesis of Mesoporous Ag₃VO₄ Powder and Its Photoluminescence Property[J]. Materials and Mechanical Engineering, 2017, 41(8): 35-39. DOI: 10.11973/jxgccl201708008

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Solvothermal Synthesis of Mesoporous Ag₃VO₄ Powder and Its Photoluminescence Property

College of Chemistry and Chemical Engineering, Qiqihar University, Qiqihar 161006, China

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Received Date: February 26, 2017
Revised Date: June 14, 2017

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Abstract

The precursor solution was prepared with AgNO₃ and NH₄VO₃ as raw materials, and solvothermal reacted at different temperatures for different times. Then the products were sintered at 600℃ and the Ag₃VO₄ powder was obtained. The morphology and phase composition of the powder were studied and the relatively optimal reaction temperature and time were determined. The structure and photoluminescence property of the powder were also analyzed. The results show that the relatively optimal reaction temperature of Ag₃VO₄ powder was 180℃ and the time was 12 h. Under this condition, the synthesized Ag₃VO₄ powder was microrod-like with the diameter of 2-3 μm. The powder had a mesoporous structure with the pore size of about 27 nm and the specific surface area of 1 181 m²·g^-1. The fluorescence emission peak of Ag₃VO₄ powder was in the wavelength range of 521-595 nm and the emission peak strength at 553.1 nm was the highest, showing a good photoluminescence property.
- Ag₃VO₄ powder,
- mesoporous,
- solvothermal synthesis,
- photoluminescence property

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[1]	雷小菊,王军,郝红, 等. 介孔材料的制备及应用研究[J]. 硅酸盐通报, 2014, 33(10):2534-2540.
[2]	许晓颖,刘明,徐国辉.合成条件对钒掺杂介孔二氧化硅结构的影响[J].洛阳理工学院学报(自然科学版),2016,26(4):12-15.
[3]	PARK M H, KIM K, KIM J, et al. Flexible dimensional control of high-capacity Li-ion-battery anodes:From 0D hollow to 3D porous germanium nanoparticle assemblies[J].Advanced Materials, 2010, 22(3):415-418.
[4]	BI H P, GUAN M, LI J C, et al. Synthesis and properties of novel functional mesoporous materials[J].Journal of Porous Materials, 2013, 20(5):1299-1304.
[5]	CLOET V, RAW A, POEPPELMEIER K R, et al. Structural, optical, and transport properties of α-and β-Ag₃VO₄[J].Chemistry of Materials,2012,24(17):3346-3354.
[6]	YAN M, WU Y, YAN Y,et al. Synthesis and characterization of novel BiVO₄/Ag₃VO₄ heterojunction with enhanced visible-light-driven photocatalytic degradation of dyes[J]. ACS Sustainable Chemistry & Engineering, 2016, 4(3):757-766.
[7]	WANG P, TANG H, AO Y,et al. In-situ growth of Ag₃VO₄ nanoparticles onto BiOCl nanosheet to form a heterojunction photocatalyst with enhanced performance under visible light irradiation[J]. Journal of Alloys & Compounds,2016,688:1-7.
[8]	BAI J, ZHOU B. Titanium dioxide nanomaterials for sensor applications[J]. Chemical Reviews, 2014, 114(19):10131-10176.
[9]	ALLAEDINI G, TASIRIN S M, AMINAYI P. Magnetic properties of cobalt ferrite synthesized by hydrothermal method[J]. International Nano Letters, 2015, 5(4):183-186.
[10]	MOULDER J F, CHASTAIN J, KING R C J. Handbook of X-ray photoelectron spectroscopy:A reference book of standard spectra for identification and interpretation of XPS data[J]. Chemical Physics Letters, 1995, 220(1):7-10.

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Solvothermal Synthesis of Mesoporous Ag3VO4 Powder and Its Photoluminescence Property

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Solvothermal Synthesis of Mesoporous Ag₃VO₄ Powder and Its Photoluminescence Property