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HAN Lei, WANG Junkai, DENG Xiangong, GE Shengtao, ZHANG Haijun. Effect of Sodium Silicate Addition Amount on Properties of Porous Diatomite Ceramics[J]. Materials and Mechanical Engineering, 2018, 42(4): 73-77. DOI: 10.11973/jxgccl201804016
Citation: HAN Lei, WANG Junkai, DENG Xiangong, GE Shengtao, ZHANG Haijun. Effect of Sodium Silicate Addition Amount on Properties of Porous Diatomite Ceramics[J]. Materials and Mechanical Engineering, 2018, 42(4): 73-77. DOI: 10.11973/jxgccl201804016

Effect of Sodium Silicate Addition Amount on Properties of Porous Diatomite Ceramics

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  • Received Date: August 01, 2017
  • Revised Date: March 11, 2018
  • Porous diatomite ceramics were prepared by foam-gelcasting method after holding at 1 000℃ for 2 h with industrial diatomite fine powder as raw material and sodium silicate as sintering aid. The addition amount (0-5wt%) of sodium silicate on the phase composition, microstructure, pore size and compressive strength of the ceramics were investigated. The results show that with increasing addition amount of sodium silicate, the cristobalite content decreased while the tridymite content increased in the porous diatomite ceramics, the sintering densification increased, the pore size showed a decreasing trend, and the compressive strength was improved. When the addition amount of sodium silicate was 3wt%, the diatomite ceramics with a hierarchically pore-structure were obtained; the compressive strength was (1.13±0.08) MPa, which increased by about 113% comparing with that without sodium silicate, and the thermal conductivity at 200℃ was (0.098±0.002) W·m-1·K-1.
  • [1]
    DA J, DU Y H, LI M D, et al. The preparation and performance study of thermal insulating materials with diatomite[J]. Advanced Materials Research, 2014, 941/942/943/944:1562-1565.
    [2]
    郑水林, 高如琴, 王健东,等. TiO2/硅藻土基多孔陶瓷复合材料的制备及降解甲醛性能[J]. 硅酸盐学报, 2008, 36(11):1633-1637.
    [3]
    LIN K L, LAN J Y, LUO K W, et al. Effects of sintering temperature on water retention characteristics of sewage sludge ash-diatomite based porous ceramics[C]//4th International Conference on Future Environment and Energy. Singapore:LACSIT Press, 2014.
    [4]
    HAN M, YIN X, KONG L, et al. Graphene-wrapped ZnO hollow spheres with enhanced electromagnetic wave absorption properties[J]. Journal of Materials Chemistry A, 2014, 2(39):16403-16409.
    [5]
    DENG X G, WANG J K, ZHANG H J, et al. Effects of firing temperature on the microstructures and properties of porous mullite ceramics prepared by foam-gelcasting[J]. Advances in Applied Ceramics, 2016, 115(4):204-209.
    [6]
    DENG X G, WANG J K, LIU J H, et al. Low cost foam-gelcasting preparation and characterization of porous magnesium aluminate spinel (MgAl2O4) ceramics[J]. Ceramics International, 2016, 42(16):18215-18222.
    [7]
    HAN Y, LI C, BIAN C, et al. Porous anorthite ceramics with ultra-low thermal conductivity[J]. Journal of the European Ceramic Society, 2013, 33(13/14):2573-2578.
    [8]
    DENG X G, WANG J K, LIU J H, et al. Preparation and characterization of porous mullite ceramics via foam-gelcasting[J]. Ceramics International, 2015, 41(7):9009-9017.
    [9]
    FANG B, KIM J H, KIM M S, et al. Hierarchical nanostructured carbons with meso-macroporosity:Design, characterization, and applications[J]. Accounts of Chemical Research, 2013, 46(7):1397-1406.
    [10]
    MILLE C, CORKERY R W. A structural and thermal conductivity study of highly porous, hierarchical polyhedral nanofoam shells made by condensing silica in microemulsion films on the surface of emulsified oil drops[J]. Journal of Materials Chemistry A, 2013, 1(5):1849-1859.
    [11]
    KOCJAN A, SHEN Z. Colloidal processing and partial sintering of high-performance porous zirconia nanoceramics with hierarchical heterogeneities[J]. Journal of the European Ceramic Society, 2013, 33(15/16):3165-3176.
    [12]
    XU B, LI Z. Paraffin/diatomite composite phase change material incorporated cement-based composite for thermal energy storage[J]. Applied Energy, 2013, 105(2):229-237.
    [13]
    ROTTMAN J, PLATT L C, SIERRA-ALVAREZ R, et al. Removal of TiO2 nanoparticles by porous media:Effect of filtration media and water chemistry[J]. Chemical Engineering Journal, 2013, 217:212-220.
    [14]
    LIN K L, LEE T C, CHANG J C, et al. Water absorption and retention of porous ceramics cosintered from waste diatomite and catalyst[J]. Environmental Progress & Sustainable Energy, 2013, 32(3):640-648.
    [15]
    LIN K L, CHANG J C, SHIE J L, et al. Characteristics of porous ceramics produced from waste diatomite and water purification sludge[J]. Environmental Engineering Science, 2012, 29(6):436-446.
    [16]
    LIU C Y, TUAN W H, CHEN S C. Preparation of porous SiC ceramics for thermal dissipation purposes[J]. Ceramics International, 2015, 41(3):4564-4568.
    [17]
    LIU J, LI Y, LI Y, et al. Effects of pore structure on thermal conductivity and strength of alumina porous ceramics using carbon black as pore-forming agent[J]. Ceramics International, 2016, 42(7):8221-8228.
    [18]
    李景华. 焦炉炭化室热补料的制备与性能研究[D]. 济南:济南大学, 2016.
    [19]
    LI C, BIAN C, HAN Y, et al. Mullite whisker reinforced porous anorthite ceramics with low thermal conductivity and high strength[J]. Journal of the European Ceramic Society, 2016, 36(3):761-765.
    [20]
    HAN L, LI F, DENG X, et al. Foam-gelcasting preparation, microstructure and thermal insulation performance of porous diatomite ceramics with hierarchical pore structures[J]. Journal of the European Ceramic Society, 2017, 37(7):2717-2725.

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